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Information card for entry 2019740
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| Coordinates | 2019740.cif |
|---|---|
| Structure factors | 2019740.hkl |
| Original IUCr paper | HTML |
| Chemical name | Poly[[aquadi-μ-cyanido-κ^4^<i>C</i>:<i>N</i>-hexacyanido-κ^6^<i>C</i>-(dimethylformamide-κ<i>O</i>)bis(3,4,7,8-tetramethyl-1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')terbium(III)molybdate(V)] 4.5-hydrate] |
|---|---|
| Formula | C86 H100 Mo2 N26 O13 Tb2 |
| Calculated formula | C86 H100 Mo2 N26 O13 Tb2 |
| Title of publication | The synthesis, crystal structure and magnetic properties of a one-dimensional terbium(III)‒octacyanidomolybdate(V) assembly |
| Authors of publication | Shen, Hong |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2014 |
| Journal volume | 70 |
| Journal issue | 12 |
| Pages of publication | 1169 - 1173 |
| a | 16.7649 ± 0.0014 Å |
| b | 13.474 ± 0.002 Å |
| c | 21.0984 ± 0.0012 Å |
| α | 90° |
| β | 96.671 ± 0.003° |
| γ | 90° |
| Cell volume | 4733.7 ± 0.9 Å3 |
| Cell temperature | 291 ± 2 K |
| Ambient diffraction temperature | 291 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0675 |
| Residual factor for significantly intense reflections | 0.0616 |
| Weighted residual factors for significantly intense reflections | 0.148 |
| Weighted residual factors for all reflections included in the refinement | 0.1488 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181867 (current) | 2016-04-06 | hkl/2/01/ (antanas@echidna) Adding IUCr specific svn headers to multiple entries in subrange 2/01/97. |
2019740.cif 2019740.hkl |
| 180865 | 2016-04-02 | cif/2/01/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01/97. |
2019740.cif 2019740.hkl |
| 176760 | 2016-02-20 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01. |
2019740.cif 2019740.hkl |
| 127939 | 2014-11-28 | cif/ hkl/ Adding structures of 2019740 via cif-deposit CGI script. |
2019740.cif 2019740.hkl |
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