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Information card for entry 2234375
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| Coordinates | 2234375.cif |
|---|---|
| Structure factors | 2234375.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis{<i>N</i>-[(diethylamino)dimethylsilyl]anilinido- κ^2^<i>N</i>,<i>N</i>'}nickel(II) |
|---|---|
| Formula | C24 H42 N4 Ni Si2 |
| Calculated formula | C24 H42 N4 Ni Si2 |
| SMILES | c1(ccccc1)N1[Ni]2([N](CC)(CC)[Si]1(C)C)N(c1ccccc1)[Si](C)(C)[N]2(CC)CC |
| Title of publication | Bis{<i>N</i>-[(diethylamino)dimethylsilyl]anilinido-κ^2^<i>N</i>,<i>N</i>'}nickel(II) |
| Authors of publication | Chen, Juan; Li, Jing |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2012 |
| Journal volume | 68 |
| Journal issue | 4 |
| Pages of publication | m357 |
| a | 21.2631 ± 0.0011 Å |
| b | 30.0347 ± 0.0016 Å |
| c | 8.6228 ± 0.0005 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 5506.8 ± 0.5 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 43 |
| Hermann-Mauguin space group symbol | F d d 2 |
| Hall space group symbol | F 2 -2d |
| Residual factor for all reflections | 0.0462 |
| Residual factor for significantly intense reflections | 0.0399 |
| Weighted residual factors for significantly intense reflections | 0.1001 |
| Weighted residual factors for all reflections included in the refinement | 0.1041 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181265 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/43. |
2234375.cif 2234375.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2234375.cif 2234375.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2234375.cif 2234375.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2234375.cif 2234375.hkl |
| 66590 | 2012-09-11 | hkl/ Adding assigned .htl files for the most recent IUCr data depositions. |
2234375.cif 2234375.hkl |
| 55648 | 2012-05-05 | cif/ Adding structures of 2234375 via cif-deposit CGI script. |
2234375.cif |
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Users of the data should acknowledge the original authors of the
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