Crystallography Open Database

Information card for entry 2311350

Preview

Coordinates	2311350.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Poly[bis(μ~3~-cyanido-κ^3^<i>C</i>:<i>C</i>:<i>N</i>)tris(μ~2~-cyanido-κ^2^<i>C</i>:<i>N</i>)bis(<i>N</i>-methylethane-1,2-diamine\- κ^2^<i>N</i>,<i>N</i>')tricopper(I)copper(II)]
Formula	C11 H20 Cu4 N9
Calculated formula	C11 H20 Cu4 N9
Title of publication	Crystal structures of two mixed-valence copper cyanide complexes with <i>N</i>-methyl-ethylenedi-amine.
Authors of publication	Corfield, Peter W. R.; Sabatino, Alexander
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2017
Journal volume	73
Journal issue	Pt 2
Pages of publication	141 - 146
a	19.509 ± 0.002 Å
b	8.2306 ± 0.0013 Å
c	11.1 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	1782.3 ± 0.5 Å³
Cell temperature	303 ± 2 K
Ambient diffraction temperature	303 ± 1 K
Number of distinct elements	4
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0189
Residual factor for significantly intense reflections	0.018
Weighted residual factors for significantly intense reflections	0.0445
Weighted residual factors for all reflections included in the refinement	0.0447
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
245816 (current)	2019-12-25	cif/ Adding structures of 2311350, 2311351 via cif-deposit CGI script.	2311350.cif