Crystallography Open Database

Information card for entry 2311533

Preview

Coordinates	2311533.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Bis(tetraethylammonium) dichloride decachlorocyclopentasilane dichloromethane disolvate
Formula	C18 H44 Cl16 N2 Si5
Calculated formula	C18 H44 Cl16 N2 Si5
Title of publication	Deca-chloro-cyclo-penta-silanes coordinated by pairs of chloride anions, with different cations, but the same solvent mol-ecules.
Authors of publication	Moxter, Maximilian; Teichmann, Julian; Lerner, Hans-Wolfram; Bolte, Michael; Wagner, Matthias
Journal of publication	Acta crystallographica. Section E, Crystallographic communications
Year of publication	2017
Journal volume	73
Journal issue	Pt 12
Pages of publication	1903 - 1907
a	10.3596 ± 0.0004 Å
b	13.9612 ± 0.0005 Å
c	16.0205 ± 0.0006 Å
α	89.959 ± 0.003°
β	72.484 ± 0.003°
γ	79.534 ± 0.003°
Cell volume	2169.29 ± 0.15 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0525
Residual factor for significantly intense reflections	0.0483
Weighted residual factors for significantly intense reflections	0.1268
Weighted residual factors for all reflections included in the refinement	0.1308
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
245962 (current)	2019-12-25	cif/ Adding structures of 2311532, 2311533 via cif-deposit CGI script.	2311533.cif