Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4030337
Preview
| Coordinates | 4030337.cif |
|---|
| Formula | C76 H68 B Cl O P4 W |
|---|---|
| Calculated formula | C76 B Cl O P4 W |
| Title of publication | Oxohalo complexes of W (V) and W (IV). The synthesis od crystal structures of [WOCl (dppe)2][BPh4], [PHMe2Ph][WOBr4(OPMe2Ph)] and [Li(OPMe2Ph)(THF)]2[WOBr4(OPMe2Ph)]2 |
| Authors of publication | Cotton, F. A.; Mandal, S. K. |
| Journal of publication | European Journal of Solid State and Inorganic Chemistry |
| Year of publication | 1991 |
| Journal volume | 28 |
| Pages of publication | 775 - 797 |
| a | 10.291 ± 0.003 Å |
| b | 24.274 ± 0.009 Å |
| c | 26.07 ± 0.01 Å |
| α | 90° |
| β | 96.09 ± 0.03° |
| γ | 90° |
| Cell volume | 6476 ± 4 Å3 |
| Ambient diffraction temperature | 294 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.074 |
| Weighted residual factors for significantly intense reflections | 0.092 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178482 (current) | 2016-03-21 | cif/4/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/03/03. |
4030337.cif |
| 128763 | 2014-12-15 | cif/ Adding structures of 4030337 via cif-deposit CGI script. |
4030337.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.