Crystallography Open Database

Information card for entry 4063503

Preview

Coordinates	4063503.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H23 Ir O4
Calculated formula	C16 H23 Ir O4
Title of publication	Unprecedented π-Bonded Rhodio- and Iridio-o-Benzoquinones as Organometallic Linkers for the Design of Chiral Octahedral Bimetallic Assemblies
Authors of publication	Moussa, Jamal; Rager, Marie Noelle; Chamoreau, Lise Marie; Ricard, Louis; Amouri, Hani
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	2
Pages of publication	397 - 404
a	7.121 ± 0.001 Å
b	13.743 ± 0.001 Å
c	8.296 ± 0.001 Å
α	90°
β	105.022 ± 0.001°
γ	90°
Cell volume	784.13 ± 0.16 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0277
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.06
Weighted residual factors for all reflections included in the refinement	0.0607
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178530 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/35.	4063503.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4063503.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4063503.cif
22805	2011-07-24	../uploads/cif-deposit/cod/cif Adding structures of 4063503 via cif-deposit CGI script.	4063503.cif