Crystallography Open Database

Information card for entry 4064503

Preview

Coordinates	4064503.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H27 F6 Ge N2 O3 Sb
Calculated formula	C24 H27 F6 Ge N2 O3 Sb
Title of publication	Lewis Base Complexes of an Enantiomeric Germanium(II) Cation Bearing a Bis(oxazoline) Ligand
Authors of publication	Arii, Hidekazu; Nakadate, Fumiya; Mochida, Kunio; Kawashima, Takayuki
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	17
Pages of publication	4471
a	15.0177 ± 0.0011 Å
b	15.0177 ± 0.0011 Å
c	23.3884 ± 0.0017 Å
α	90°
β	90°
γ	90°
Cell volume	5274.8 ± 0.7 Å³
Cell temperature	123 K
Ambient diffraction temperature	123 K
Number of distinct elements	7
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.0316
Residual factor for significantly intense reflections	0.0257
Weighted residual factors for significantly intense reflections	0.054
Weighted residual factors for all reflections included in the refinement	0.0561
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178539 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/45.	4064503.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064503.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064503.cif
32931	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064502, 4064503, 4064504, 4064505, 4064506 via cif-deposit CGI script.	4064503.cif