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Information card for entry 4065627
Preview
| Coordinates | 4065627.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C H1.5 Cl2.5 Si |
|---|---|
| Calculated formula | C H1.5 Cl2.5 Si |
| Title of publication | [Bu4P]+Cl−-Catalyzed Reactions of Trichlorosilane and Dichloromethylsilane with Vinyltrichlorosilane: New Synthetic Method for 1,1,4,4-Tetrachloro-2,5-bis(trichlorosilyl)-1,4-disilacyclohexane Compounds |
| Authors of publication | Hong, Soon Hyun; Hyun, Sang Il; Jung, Il Nam; Han, Won-Sik; Kim, Min-Hye; Yun, Hoseop; Nam, Suk-Woo; Kang, Sang Ook |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 13 |
| Pages of publication | 3054 |
| a | 6.1896 ± 0.0005 Å |
| b | 8.3969 ± 0.0007 Å |
| c | 9.0412 ± 0.0009 Å |
| α | 89.363 ± 0.003° |
| β | 80.569 ± 0.003° |
| γ | 78.809 ± 0.002° |
| Cell volume | 454.63 ± 0.07 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0447 |
| Residual factor for significantly intense reflections | 0.0394 |
| Weighted residual factors for significantly intense reflections | 0.1067 |
| Weighted residual factors for all reflections included in the refinement | 0.1103 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.163 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4065627.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4065627.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4065627.cif |
| 33631 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4065627, 4065628 via cif-deposit CGI script. |
4065627.cif |
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Users of the data should acknowledge the original authors of the
structural data.