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Information card for entry 4065733
Preview
| Coordinates | 4065733.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C39 H55 Dy I2 N2 O2 P2 Si2 |
|---|---|
| Calculated formula | C39 H55 Dy I2 N2 O2 P2 Si2 |
| SMILES | [Dy]12(C(P(c3ccccc3)(c3ccccc3)=[N]1[Si](C)(C)C)P(c1ccccc1)(c1ccccc1)=[N]2[Si](C)(C)C)(I)(I)[O]1CCCC1.O1CCCC1 |
| Title of publication | Synthesis and Characterization of Dysprosium and Lanthanum Bis(iminophosphorano)methanide and -methanediide Complexes |
| Authors of publication | Wooles, Ashley J.; Cooper, Oliver J.; McMaster, Jonathan; Lewis, William; Blake, Alexander J.; Liddle, Stephen T. |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 10 |
| Pages of publication | 2315 |
| a | 16.1968 ± 0.001 Å |
| b | 19.5258 ± 0.0013 Å |
| c | 14.2928 ± 0.0009 Å |
| α | 90° |
| β | 99.386 ± 0.002° |
| γ | 90° |
| Cell volume | 4459.7 ± 0.5 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0538 |
| Residual factor for significantly intense reflections | 0.0342 |
| Weighted residual factors for significantly intense reflections | 0.0743 |
| Weighted residual factors for all reflections included in the refinement | 0.0799 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.981 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178550 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/57. |
4065733.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4065733.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4065733.cif |
| 33673 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4065733, 4065734, 4065735, 4065736, 4065737 via cif-deposit CGI script. |
4065733.cif |
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Users of the data should acknowledge the original authors of the
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