Crystallography Open Database

Information card for entry 4065830

Preview

Coordinates	4065830.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H51 N3 Si4 Zn2
Calculated formula	C26 H51 N3 Si4 Zn2
SMILES	[Zn]123([Zn]4([N]2(Cc2[n]1cccc2)Cc1[n]4cccc1)(C([Si](C)(C)C)[Si](C)(C)C)[H]3)C([Si](C)(C)C)[Si](C)(C)C
Title of publication	Synthesis and Catalytic Reactivity of Bis(alkylzinc)-hydride-di(2-pyridylmethyl)amides
Authors of publication	Kahnes, Marcel; Görls, Helmar; González, Leticia; Westerhausen, Matthias
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	14
Pages of publication	3098
a	9.1445 ± 0.0003 Å
b	13.1954 ± 0.0004 Å
c	16.4616 ± 0.0005 Å
α	71.47 ± 0.002°
β	75.791 ± 0.002°
γ	70.081 ± 0.002°
Cell volume	1749.6 ± 0.1 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0691
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.0866
Weighted residual factors for all reflections included in the refinement	0.0959
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178551 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/58.	4065830.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065830.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065830.cif
33701	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065827, 4065828, 4065829, 4065830 via cif-deposit CGI script.	4065830.cif