Crystallography Open Database

Information card for entry 4065846

Preview

Coordinates	4065846.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H61 Ga Li N2 O2
Calculated formula	C37 H61 Ga Li N2 O2
Title of publication	Group 2 and 12 Metal Gallyl Complexes Containing Unsupported Ga−M Covalent Bonds (M = Mg, Ca, Sr, Ba, Zn, Cd)†
Authors of publication	Bonello, Owen; Jones, Cameron; Stasch, Andreas; Woodul, William D.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	21
Pages of publication	4914
a	19.219 ± 0.004 Å
b	10.009 ± 0.002 Å
c	21.274 ± 0.004 Å
α	90°
β	113.13 ± 0.03°
γ	90°
Cell volume	3763.4 ± 1.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0851
Residual factor for significantly intense reflections	0.0492
Weighted residual factors for significantly intense reflections	0.1065
Weighted residual factors for all reflections included in the refinement	0.1214
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178551 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/58.	4065846.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4065846.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4065846.cif
33704	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4065836, 4065837, 4065838, 4065839, 4065840, 4065841, 4065842, 4065843, 4065844, 4065845, 4065846 via cif-deposit CGI script.	4065846.cif