Crystallography Open Database

Information card for entry 4066032

Preview

Coordinates	4066032.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35.25 H50.25 Cl Pt S3 Si
Calculated formula	C35.25 H45 Cl Pt S3 Si
Title of publication	Synthesis and Complexation of a New Tripodal Tetradentate Ligand, a Silyl Ligand Tethered with Three Thioether Moieties
Authors of publication	Takeda, Nobuhiro; Watanabe, Daisuke; Nakamura, Tetsu; Unno, Masafumi
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	13
Pages of publication	2839
a	11.1478 ± 0.0008 Å
b	18.9318 ± 0.0017 Å
c	19.6732 ± 0.0017 Å
α	109.292 ± 0.002°
β	100.757 ± 0.0019°
γ	97.736 ± 0.0018°
Cell volume	3762.7 ± 0.5 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0719
Residual factor for significantly intense reflections	0.0692
Weighted residual factors for significantly intense reflections	0.1286
Weighted residual factors for all reflections included in the refinement	0.1296
Goodness-of-fit parameter for all reflections included in the refinement	1.327
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178504 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/60.	4066032.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066032.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066032.cif
33760	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066030, 4066031, 4066032, 4066033 via cif-deposit CGI script.	4066032.cif