Crystallography Open Database

Information card for entry 4066677

Preview

Coordinates	4066677.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C103 H129 N6 S4 Si2
Calculated formula	C103 H129 N6 S4 Si2
Title of publication	Synthesis and Reactivity of a Base-Free N-Heterocyclic Silanimine†
Authors of publication	Kong, Lingbing; Cui, Chunming
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	22
Pages of publication	5738
a	10.9167 ± 0.0019 Å
b	19.022 ± 0.003 Å
c	23.425 ± 0.003 Å
α	89.86 ± 0.013°
β	83.91 ± 0.009°
γ	74.496 ± 0.012°
Cell volume	4659.2 ± 1.3 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0705
Residual factor for significantly intense reflections	0.0558
Weighted residual factors for significantly intense reflections	0.1383
Weighted residual factors for all reflections included in the refinement	0.147
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178558 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/66.	4066677.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066677.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066677.cif
33957	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066677 via cif-deposit CGI script.	4066677.cif