Crystallography Open Database

Information card for entry 4066715

Preview

Coordinates	4066715.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33.81 H58.81 N4 O0.81 P Si4 Sn2
Calculated formula	C33.803 H58.803 N4 O0.803 P Si4 Sn2
Title of publication	Coordination Site SelectiveJanus HeadLigands†
Authors of publication	Objartel, Ina; Pott, Nils A.; John, Michael; Stalke, Dietmar
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	21
Pages of publication	5670
a	10.253 ± 0.0013 Å
b	14.563 ± 0.0019 Å
c	16.547 ± 0.003 Å
α	111.731 ± 0.003°
β	97.66 ± 0.003°
γ	106.814 ± 0.002°
Cell volume	2115.2 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0251
Residual factor for significantly intense reflections	0.0192
Weighted residual factors for significantly intense reflections	0.0409
Weighted residual factors for all reflections included in the refinement	0.043
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178559 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/67.	4066715.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066715.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066715.cif
33968	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066713, 4066714, 4066715 via cif-deposit CGI script.	4066715.cif