Crystallography Open Database

Information card for entry 4066733

Preview

Coordinates	4066733.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H33 Cl O2 P2 Pt
Calculated formula	C24 H33 Cl O2 P2 Pt
Title of publication	Steric Control in the Synthesis of Phosphinous Acid-Coordinated Mono- and Binuclear Platinum(II) Complexes
Authors of publication	Achard, Thierry; Giordano, Laurent; Tenaglia, Alphonse; Gimbert, Yves; Buono, Gérard
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	17
Pages of publication	3936
a	9.2775 ± 0.0003 Å
b	11.7432 ± 0.0003 Å
c	12.7385 ± 0.0003 Å
α	71.5854 ± 0.0009°
β	86.316 ± 0.001°
γ	78.548 ± 0.002°
Cell volume	1290.55 ± 0.06 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0901
Residual factor for significantly intense reflections	0.0547
Weighted residual factors for significantly intense reflections	0.127
Weighted residual factors for all reflections included in the refinement	0.149
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178559 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/67.	4066733.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066733.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066733.cif
33971	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066730, 4066731, 4066732, 4066733, 4066734, 4066735, 4066736 via cif-deposit CGI script.	4066733.cif