Crystallography Open Database

Information card for entry 4067150

Preview

Coordinates	4067150.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H45 Cl4 P Ru2 S2
Calculated formula	C38 H44 Cl4 P Ru2 S2
Title of publication	Preparation of Thiolate-Bridged Dinuclear Ruthenium Complexes Bearing a Phosphine Ligand and Application to Propargylic Reduction of Propargylic Alcohols with 2-Propanol
Authors of publication	Yuki, Masahiro; Miyake, Yoshihiro; Nishibayashi, Yoshiaki
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	22
Pages of publication	5994
a	11.0649 ± 0.0008 Å
b	14.2485 ± 0.0013 Å
c	11.7148 ± 0.0009 Å
α	90°
β	96.237 ± 0.003°
γ	90°
Cell volume	1836 ± 0.3 Å³
Cell temperature	173 ± 1 K
Ambient diffraction temperature	173 ± 1 K
Number of distinct elements	6
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0456
Residual factor for significantly intense reflections	0.0401
Weighted residual factors for significantly intense reflections	0.107
Weighted residual factors for all reflections included in the refinement	0.1115
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178562 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/71.	4067150.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067150.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067150.cif
34094	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067147, 4067148, 4067149, 4067150, 4067151, 4067152, 4067153, 4067154 via cif-deposit CGI script.	4067150.cif