Crystallography Open Database

Information card for entry 4067296

Preview

Coordinates	4067296.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	bis((N,N'-dimethylethylenediamido)-(s-butyl)-zinc)
Formula	C16 H40 N4 Zn2
Calculated formula	C16 H40 N4 Zn2
Title of publication	Toward Total Spontaneous Resolution ofsec-Butylzinc Complexes
Authors of publication	Lennartson, Anders; Hedström, Anna; Håkansson, Mikael
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	1
Pages of publication	177
a	11.998 ± 0.004 Å
b	7.218 ± 0.003 Å
c	12.46 ± 0.004 Å
α	90°
β	99.112 ± 0.011°
γ	90°
Cell volume	1065.4 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0599
Residual factor for significantly intense reflections	0.0496
Weighted residual factors for significantly intense reflections	0.1204
Weighted residual factors for all reflections included in the refinement	0.1263
Goodness-of-fit parameter for all reflections included in the refinement	0.965
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178563 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/72.	4067296.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4067296.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4067296.cif
34151	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4067291, 4067292, 4067293, 4067294, 4067295, 4067296, 4067297, 4067298 via cif-deposit CGI script.	4067296.cif