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Information card for entry 4070671
Preview
| Coordinates | 4070671.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C79 H123 K La N4 O4 |
|---|---|
| Calculated formula | C74 H112 K La N4 O4 |
| SMILES | [La]12(N(c3c(cccc3C(C)C)C(C)C)C(C)=CC(N1c1c(cccc1C(C)C)C(C)C)=C)N(c1c(cccc1C(C)C)C(C)C)C(C)=CC(=C)N2c1c(cccc1C(C)C)C(C)C.[K]([O]1CCCC1)([O]1CCCC1)([O]1CCCC1)[O]1CCCC1 |
| Title of publication | Strategies for the Synthesis of Lanthanum Dialkyl Complexes with Monoanionic Ancillary Ligands |
| Authors of publication | Bambirra, Sergio; Perazzolo, Francesca; Boot, Steven J.; Sciarone, Timo J. J.; Meetsma, Auke; Hessen, Bart |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 4 |
| Pages of publication | 704 |
| a | 21.519 ± 0.003 Å |
| b | 14.637 ± 0.002 Å |
| c | 48.082 ± 0.007 Å |
| α | 90° |
| β | 96.458 ± 0.002° |
| γ | 90° |
| Cell volume | 15048 ± 4 Å3 |
| Cell temperature | 100 ± 1 K |
| Ambient diffraction temperature | 100 ± 1 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.1112 |
| Residual factor for significantly intense reflections | 0.0911 |
| Weighted residual factors for significantly intense reflections | 0.1685 |
| Weighted residual factors for all reflections included in the refinement | 0.1753 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.255 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178595 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/06. |
4070671.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4070671.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4070671.cif |
| 42633 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4070671 via cif-deposit CGI script. |
4070671.cif |
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Users of the data should acknowledge the original authors of the
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