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Information card for entry 4070739
Preview
| Coordinates | 4070739.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H46 Li N O Si2 |
|---|---|
| Calculated formula | C23 H46 Li N O Si2 |
| SMILES | [Si](C([Si](C)(C)C)N(c1c(cccc1C(C)C)C(C)C)[Li][O](CC)CC)(C)(C)C |
| Title of publication | Synthesis and Characterization of the Monomeric Vicinal Dianion Li~2~(THF)~3~[ArNC(SiMe~3~)~2~] and the Aluminum and Lithium Derivatives of the Amido Ligand [ArNCH(SiMe~3~)~2~]^-^ |
| Authors of publication | Cheng, Xiaoyan; Zhang, Jianying; Song, Haibin; Cui, Chunming |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 4 |
| Pages of publication | 678 - 682 |
| a | 9.9324 ± 0.0012 Å |
| b | 17.397 ± 0.002 Å |
| c | 16.0983 ± 0.0018 Å |
| α | 90° |
| β | 101.203 ± 0.002° |
| γ | 90° |
| Cell volume | 2728.7 ± 0.5 Å3 |
| Cell temperature | 113 ± 2 K |
| Ambient diffraction temperature | 113 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0658 |
| Residual factor for significantly intense reflections | 0.0498 |
| Weighted residual factors for significantly intense reflections | 0.1104 |
| Weighted residual factors for all reflections included in the refinement | 0.1179 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 209848 (current) | 2018-08-17 | cif/4/ Updating bibliography in entries 4070735-4070739, 4083494. Marking entry 4083494 as a duplicat of entry 4070735. |
4070739.cif |
| 178596 | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/07. |
4070739.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4070739.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4070739.cif |
| 42667 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4070739 via cif-deposit CGI script. |
4070739.cif |
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Users of the data should acknowledge the original authors of the
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