Crystallography Open Database

Information card for entry 4070830

Preview

Coordinates	4070830.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H66 B F24 N3 Pd
Calculated formula	C66 H66 B F24 N3 Pd
Title of publication	Reactions of Cationic Palladium α-Diimine Complexes with Nitrogen-Containing Olefins: Branched Polyethylene with Carbazole Functionalities
Authors of publication	Li, Weidong; Zhang, Xiaochun; Meetsma, Auke; Hessen, Bart
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	9
Pages of publication	2052
a	41.414 ± 0.002 Å
b	12.7965 ± 0.0005 Å
c	26.01 ± 0.001 Å
α	90°
β	103 ± 0.001°
γ	90°
Cell volume	13430.8 ± 1 Å³
Cell temperature	100 ± 1 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0989
Residual factor for significantly intense reflections	0.0618
Weighted residual factors for significantly intense reflections	0.1468
Weighted residual factors for all reflections included in the refinement	0.1664
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4070830.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070830.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070830.cif
42729	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070830 via cif-deposit CGI script.	4070830.cif