Crystallography Open Database

Information card for entry 4070852

Preview

Coordinates	4070852.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27.5 H45 Cl4 N6 O14.5 Pd2
Calculated formula	C27.5 H45 Cl4 N6 O14.5 Pd2
Title of publication	Synthesis of Bis(2,6-dinitroaryl)palladium(II) and Mono(2,6-dinitroaryl)platinum(II) Complexes. A New Example of the Transphobia Effect and of Transmetalation from Pt to Hg
Authors of publication	Vicente, José; Arcas, Aurelia; Gálvez-López, María-Dolores; Juliá-Hernández, Francisco; Bautista, Delia; Jones, Peter G.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	7
Pages of publication	1582
a	14.6377 ± 0.0006 Å
b	16.8923 ± 0.0007 Å
c	18.0811 ± 0.0007 Å
α	73.573 ± 0.002°
β	88.311 ± 0.002°
γ	71.063 ± 0.002°
Cell volume	4046.6 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0636
Residual factor for significantly intense reflections	0.0424
Weighted residual factors for significantly intense reflections	0.0913
Weighted residual factors for all reflections included in the refinement	0.1006
Goodness-of-fit parameter for all reflections included in the refinement	1.017
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4070852.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070852.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070852.cif
42767	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070852 via cif-deposit CGI script.	4070852.cif