Crystallography Open Database

Information card for entry 4070978

Preview

Coordinates	4070978.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H35 N6 Nb
Calculated formula	C12 H12 N6 Nb
Title of publication	Unexpected Formation of (Dimethylaminomethylene)methylamide Complexes from the Reactions between Metal Chlorides and Lithium Dimethylamide
Authors of publication	Zhang, Xin-Hao; Chen, Shu-Jian; Cai, Hu; Im, Hee-Jung; Chen, Tianniu; Yu, Xianghua; Chen, Xuetai; Lin, Zhenyang; Wu, Yun-Dong; Xue, Zi-Ling
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	6
Pages of publication	1338
a	9.852 ± 0.0011 Å
b	9.852 ± 0.0011 Å
c	9.852 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	956.25 ± 0.18 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	229
Hermann-Mauguin space group symbol	I m -3 m
Hall space group symbol	-I 4 2 3
Residual factor for all reflections	0.0465
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.1123
Weighted residual factors for all reflections included in the refinement	0.1123
Goodness-of-fit parameter for all reflections included in the refinement	1.192
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178598 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/09.	4070978.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070978.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070978.cif
42941	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070978 via cif-deposit CGI script.	4070978.cif