Crystallography Open Database

Information card for entry 4071202

Preview

Coordinates	4071202.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	complex 4
Formula	C22 H40 Cl O2 P2 Rh
Calculated formula	C22 H40 Cl O2 P2 Rh
Title of publication	B−C Bond Cleavage of BArFAnion Upon Oxidation of Rhodium(I) with AgBArF. Phosphinite Rhodium(I), Rhodium(II), and Rhodium(III) Pincer Complexes
Authors of publication	Salem, Hiyam; Shimon, Linda J. W.; Leitus, Gregory; Weiner, Lev; Milstein, David
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	10
Pages of publication	2293
a	8.176 ± 0.0016 Å
b	12.184 ± 0.002 Å
c	13.351 ± 0.003 Å
α	100.49 ± 0.03°
β	95.71 ± 0.03°
γ	103.91 ± 0.03°
Cell volume	1255 ± 0.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0286
Residual factor for significantly intense reflections	0.0261
Weighted residual factors for significantly intense reflections	0.062
Weighted residual factors for all reflections included in the refinement	0.0633
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178601 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/12.	4071202.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071202.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071202.cif
43102	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4071200, 4071201, 4071202 via cif-deposit CGI script.	4071202.cif