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Information card for entry 4071612
Preview
| Coordinates | 4071612.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C58 H84 Ge2 N4 P2 |
|---|---|
| Calculated formula | C58 H84 Ge2 N4 P2 |
| SMILES | CC1=CC(C)=[N](c2c(cccc2C(C)C)C(C)C)[Ge](N1c1c(C(C)C)cccc1C(C)C)PP[Ge]1N(C(=CC(C)=[N]1c1c(cccc1C(C)C)C(C)C)C)c1c(cccc1C(C)C)C(C)C |
| Title of publication | Facile Access to a Stable Divalent Germanium Compound with a Terminal PH2Group and Related PR2Derivatives |
| Authors of publication | Yao, Shenglai; Brym, Markus; Merz, Klaus; Driess, Matthias |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 14 |
| Pages of publication | 3601 |
| a | 10.8175 ± 0.0006 Å |
| b | 12.0783 ± 0.0007 Å |
| c | 12.6434 ± 0.0007 Å |
| α | 91.55 ± 0.002° |
| β | 108.361 ± 0.002° |
| γ | 111.339 ± 0.002° |
| Cell volume | 1441.49 ± 0.14 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1493 |
| Residual factor for significantly intense reflections | 0.0721 |
| Weighted residual factors for significantly intense reflections | 0.1427 |
| Weighted residual factors for all reflections included in the refinement | 0.1739 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.963 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178605 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/16. |
4071612.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4071612.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4071612.cif |
| 43946 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4071609, 4071610, 4071611, 4071612, 4071613 via cif-deposit CGI script. |
4071612.cif |
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Users of the data should acknowledge the original authors of the
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