Crystallography Open Database

Information card for entry 4071733

Preview

Coordinates	4071733.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H40 Cl2 F3 O3 P Ru2 S
Calculated formula	C25 H40 Cl2 F3 O3 P Ru2 S
Title of publication	Novel Monophosphido-Bridged Diruthenium Complexes: Efficient Preparative Method and Catalytic Activity toward Reactions of Propargylic Alcohols with Aromatic Compounds
Authors of publication	Miyake, Yoshihiro; Endo, Satoshi; Nomaguchi, Yohei; Yuki, Masahiro; Nishibayashi, Yoshiaki
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	15
Pages of publication	4017
a	19.1907 ± 0.0004 Å
b	19.1907 ± 0.0004 Å
c	16.3113 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	6007.2 ± 0.2 Å³
Cell temperature	173.1 K
Number of distinct elements	8
Space group number	86
Hermann-Mauguin space group symbol	P 42/n :2
Hall space group symbol	-P 4bc
Residual factor for significantly intense reflections	0.0223
Weighted residual factors for all reflections included in the refinement	0.0497
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4071733.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071733.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071733.cif
44004	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071732, 4071733 via cif-deposit CGI script.	4071733.cif