Crystallography Open Database

Information card for entry 4071753

Preview

Coordinates	4071753.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H41 Cl2 Fe Si
Calculated formula	C34 H41 Cl2 Fe Si
Title of publication	1,2-Bis(ferrocenyl)disilene: A Multistep Redox System with an SiSi Double Bond
Authors of publication	Sasamori, Takahiro; Yuasa, Akihiro; Hosoi, Yoshinobu; Furukawa, Yukio; Tokitoh, Norihiro
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	14
Pages of publication	3325
a	9.2204 ± 0.0002 Å
b	12.5311 ± 0.0003 Å
c	15.1144 ± 0.0004 Å
α	70.815 ± 0.0018°
β	80.039 ± 0.001°
γ	69.2381 ± 0.001°
Cell volume	1539.09 ± 0.07 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0364
Residual factor for significantly intense reflections	0.0293
Weighted residual factors for significantly intense reflections	0.0719
Weighted residual factors for all reflections included in the refinement	0.0759
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178606 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/17.	4071753.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4071753.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4071753.cif
44013	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4071753 via cif-deposit CGI script.	4071753.cif