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Information card for entry 4072073
Preview
| Coordinates | 4072073.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H42 Cl O2 P Pd |
|---|---|
| Calculated formula | C22 H42 Cl O2 P Pd |
| SMILES | [Pd]([C@@H]1[C@@H]([C@H]2[C@H](C[C@@H]1C2)C(=O)OC)C)(Cl)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C.[Pd]([C@H]1[C@H]([C@@H]2[C@@H](C[C@H]1C2)C(=O)OC)C)(Cl)[P](C(C)(C)C)(C(C)(C)C)C(C)(C)C |
| Title of publication | Syntheses of Ester-Substituted Norbornyl Palladium Complexes Ligated withtBu3P: Studies on the Insertion ofexo- andendo-Monomers in the Ester-Substituted Norbornene Polymerization |
| Authors of publication | Takamiya, Ikuko; Yamashita, Makoto; Nozaki, Kyoko |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 20 |
| Pages of publication | 5347 |
| a | 8.592 ± 0.005 Å |
| b | 10.019 ± 0.005 Å |
| c | 15.068 ± 0.008 Å |
| α | 100.372 ± 0.006° |
| β | 100.796 ± 0.006° |
| γ | 104.467 ± 0.006° |
| Cell volume | 1198.1 ± 1.1 Å3 |
| Cell temperature | 103.15 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.025 |
| Residual factor for significantly intense reflections | 0.0236 |
| Weighted residual factors for significantly intense reflections | 0.0598 |
| Weighted residual factors for all reflections included in the refinement | 0.0606 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178609 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/20. |
4072073.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4072073.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4072073.cif |
| 44215 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4072073 via cif-deposit CGI script. |
4072073.cif |
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Users of the data should acknowledge the original authors of the
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