Crystallography Open Database

Information card for entry 4072089

4072088 << 4072089 >> 4072090

Preview

Coordinates	4072089.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H33 N2 O10 Os4
Calculated formula	C40 H33 N2 O10 Os4
Title of publication	NHC Complexes of Osmium Clusters: A Structural and Reactivity Study
Authors of publication	Cooke, Craig E.; Jennings, Michael C.; Katz, Michael J.; Pomeroy, R. K.; Clyburne, Jason A. C.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	22
Pages of publication	5777
a	12.3074 ± 0.0004 Å
b	12.6819 ± 0.0004 Å
c	14.7598 ± 0.0005 Å
α	74.792 ± 0.002°
β	87.235 ± 0.002°
γ	62.317 ± 0.002°
Cell volume	1961.26 ± 0.12 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0552
Residual factor for significantly intense reflections	0.0513
Weighted residual factors for significantly intense reflections	0.1408
Weighted residual factors for all reflections included in the refinement	0.1448
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178609 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/20.	4072089.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072089.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072089.cif
44226	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072089 via cif-deposit CGI script.	4072089.cif