Crystallography Open Database

Information card for entry 4072286

Preview

Coordinates	4072286.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26.5 H36 Cl3 N3 Ru
Calculated formula	C26.5 H36 Cl3 N3 Ru
Title of publication	Unsymmetrical Bis(iminoethyl)pyridine Metal Complexes with a Pendant Alkenyl Substituent. Part B: Internal Olefin Coordination to Ruthenium†
Authors of publication	Wallenhorst, Carolin; Kehr, Gerald; Fröhlich, Roland; Erker, Gerhard
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	24
Pages of publication	6557
a	25.836 ± 0.001 Å
b	10.897 ± 0.001 Å
c	19.487 ± 0.001 Å
α	90°
β	96.4 ± 0.01°
γ	90°
Cell volume	5452.1 ± 0.6 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0611
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.1472
Weighted residual factors for all reflections included in the refinement	0.1548
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4072286.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072286.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072286.cif
44329	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072286 via cif-deposit CGI script.	4072286.cif