Crystallography Open Database

Information card for entry 4072967

Preview

Coordinates	4072967.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H60 O3 Si6 Yb
Calculated formula	C24 H60 O3 Si6 Yb
SMILES	[Yb]123([O]([Si](C)(C)[C@@]2([Si](C)(C)CC[Si]([C@@]3([Si](C)(C)C)[Si]([O]1C)(C)C)(C)C)[Si](C)(C)C)C)[O]1CCCC1
Title of publication	Synthesis and Structures of Ln(II) and Ln(III) Dialkyls Derived from LnI2(Ln = Nd, Tm, Yb)
Authors of publication	Bowman, Lyndsey J.; Izod, Keith; Clegg, William; Harrington, Ross W.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	10
Pages of publication	2646
a	12.7912 ± 0.0006 Å
b	16.5615 ± 0.0008 Å
c	16.8787 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	3575.6 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0356
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.0811
Weighted residual factors for all reflections included in the refinement	0.0822
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.6771 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178618 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/29.	4072967.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072967.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072967.cif
46088	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072966, 4072967, 4072968, 4072969 via cif-deposit CGI script.	4072967.cif