Crystallography Open Database

Information card for entry 4073035

Preview

Coordinates	4073035.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H0 Br Dy K O6
Calculated formula	C58 H106 Br Dy K O6
Title of publication	Isolation of Stable Organodysprosium(II) Complexes by Chemical Reduction of Dysprosium(III) Precursors
Authors of publication	Jaroschik, Florian; Nief, François; Le Goff, Xavier-Frédéric; Ricard, Louis
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	5
Pages of publication	1123
a	13.172 ± 0.001 Å
b	19.112 ± 0.001 Å
c	25.098 ± 0.001 Å
α	90°
β	97.218 ± 0.001°
γ	90°
Cell volume	6268.2 ± 0.6 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0452
Weighted residual factors for significantly intense reflections	0.1129
Weighted residual factors for all reflections included in the refinement	0.1234
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178619 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/30.	4073035.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073035.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073035.cif
46127	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073029, 4073030, 4073031, 4073032, 4073033, 4073034, 4073035 via cif-deposit CGI script.	4073035.cif