Crystallography Open Database

Information card for entry 4073290

Preview

Coordinates	4073290.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H47 Cl3 F8 N4 O
Calculated formula	C54 H47 Cl3 F8 N4 O
Title of publication	Dinuclear Zinc Complexes Based on Parallel β-Diiminato Binding Sites: Syntheses, Structures, and Properties as CO2/Epoxide Copolymerization Catalysts
Authors of publication	Pilz, Maurice Frederic; Limberg, Christian; Lazarov, Boyan B.; Hultzsch, Kai C.; Ziemer, Burkhard
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	15
Pages of publication	3668
a	16.073 ± 0.005 Å
b	16.716 ± 0.005 Å
c	18.411 ± 0.007 Å
α	90°
β	90°
γ	90°
Cell volume	4947 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	52
Hermann-Mauguin space group symbol	P n n a
Hall space group symbol	-P 2a 2bc
Residual factor for all reflections	0.1339
Residual factor for significantly intense reflections	0.1134
Weighted residual factors for significantly intense reflections	0.2277
Weighted residual factors for all reflections included in the refinement	0.2388
Goodness-of-fit parameter for all reflections included in the refinement	1.213
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178621 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/32.	4073290.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4073290.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4073290.cif
46270	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4073289, 4073290, 4073291, 4073292, 4073293 via cif-deposit CGI script.	4073290.cif