Crystallography Open Database

Information card for entry 4074158

Preview

Coordinates	4074158.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H40 O4 Zn4
Calculated formula	C16 H44 O4 Zn4
Title of publication	Convenient Access to Homo- and Heterobimetallic Alkoxo Hydridozinc Clusters of Formula [(HZnOtBu)4-n(LiOtBu)n] (n= 0, 1, 2, 3)
Authors of publication	Marciniak, Wojciech; Merz, Klaus; Moreno, Mariluna; Driess, Matthias
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	21
Pages of publication	4931
a	18.0127 ± 0.0007 Å
b	9.3522 ± 0.0004 Å
c	20.0134 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	3371.4 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	63
Hermann-Mauguin space group symbol	C m c m
Hall space group symbol	-C 2c 2
Residual factor for all reflections	0.0529
Residual factor for significantly intense reflections	0.0459
Weighted residual factors for significantly intense reflections	0.1053
Weighted residual factors for all reflections included in the refinement	0.108
Goodness-of-fit parameter for all reflections included in the refinement	1.133
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178630 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/41.	4074158.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074158.cif
48231	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074158, 4074159, 4074160, 4074161 via cif-deposit CGI script.	4074158.cif