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Information card for entry 4074227
Preview
| Coordinates | 4074227.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | (K-crypt)3[Ge9Zn(C6H5)]*2en*tol |
|---|---|
| Formula | C71 H137 Ge9 K3 N10 O18 Zn |
| Calculated formula | C71 H111.01 Ge9 K3 N10 O18 Zn |
| Title of publication | Organozinc Derivatives of Deltahedral Zintl Ions: Synthesis and Characterization ofcloso-[E9Zn(C6H5)]3-(E = Si, Ge, Sn, Pb) |
| Authors of publication | Goicoechea, Jose M.; Sevov, Slavi C. |
| Journal of publication | Organometallics |
| Year of publication | 2006 |
| Journal volume | 25 |
| Journal issue | 19 |
| Pages of publication | 4530 |
| a | 13.8684 ± 0.0004 Å |
| b | 14.9256 ± 0.0004 Å |
| c | 25.9765 ± 0.0007 Å |
| α | 76.627 ± 0.002° |
| β | 84.302 ± 0.002° |
| γ | 68.919 ± 0.002° |
| Cell volume | 4880.3 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0647 |
| Residual factor for significantly intense reflections | 0.0488 |
| Weighted residual factors for significantly intense reflections | 0.1434 |
| Weighted residual factors for all reflections included in the refinement | 0.1549 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.092 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178631 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/42. |
4074227.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4074227.cif |
| 48261 | 2012-03-26 | ../uploads/cif-deposit/cod/cif Adding structures of 4074226, 4074227, 4074228, 4074229 via cif-deposit CGI script. |
4074227.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.