Crystallography Open Database

Information card for entry 4074265

Preview

Coordinates	4074265.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H47 Mo2 O4 P Sn
Calculated formula	C44 H47 Mo2 O4 P Sn
Title of publication	Dimolybdenum−Tin Derivatives of the Unsaturated Hydride [Mo2(η5-C5H5)2(μ-H)(μ-PCy2)(CO)2] and HSnR3(R = Ph, Bu): Bridging versus Terminal Coordination of the Triorganostannyl Group
Authors of publication	Alvarez, M. Angeles; García, M. Esther; Ramos, Alberto; Ruiz, Miguel A.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	22
Pages of publication	5374
a	11.7278 ± 0.0019 Å
b	14.627 ± 0.002 Å
c	22.86 ± 0.004 Å
α	90°
β	97.054 ± 0.003°
γ	90°
Cell volume	3891.8 ± 1.1 Å³
Cell temperature	120 ± 0.1 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1584
Residual factor for significantly intense reflections	0.0608
Weighted residual factors for significantly intense reflections	0.1156
Weighted residual factors for all reflections included in the refinement	0.1581
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178631 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/42.	4074265.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074265.cif
48275	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074264, 4074265 via cif-deposit CGI script.	4074265.cif