Crystallography Open Database

Information card for entry 4074283

Preview

Coordinates	4074283.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H82 Ag B33 O4 Sn2
Calculated formula	C47 H82 Ag B33 O4 Sn2
Title of publication	Stabilization of Triaryltin(IV) Cations Containing an O,C,O-Coordinating Pincer-Type Ligand. Isolation of a New [Ag(1-CB11H12)3]2-Anion
Authors of publication	Kašná, Blanka; Jambor, Roman; Dostál, Libor; Císařová, Ivana; Holeček, Jaroslav; Štíbr, Bohumil
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	21
Pages of publication	5139
a	14.644 ± 0.0001 Å
b	20.529 ± 0.0002 Å
c	22.644 ± 0.0002 Å
α	90°
β	104.403 ± 0.0004°
γ	90°
Cell volume	6593.44 ± 0.1 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0335
Residual factor for significantly intense reflections	0.0285
Weighted residual factors for significantly intense reflections	0.0728
Weighted residual factors for all reflections included in the refinement	0.0757
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178631 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/42.	4074283.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074283.cif
48286	2012-03-26	../uploads/cif-deposit/cod/cif Adding structures of 4074283, 4074284, 4074285 via cif-deposit CGI script.	4074283.cif