Crystallography Open Database

Information card for entry 4075725

Preview

Coordinates	4075725.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H42 Hf N4 P2
Calculated formula	C18 H42 Hf N4 P2
Title of publication	Bis(amido)cyclodiphosph(III)azane Hafnium Complexes and Their Activation by Tris(perfluorophenyl)borane
Authors of publication	Axenov, Kirill V.; Klinga, Martti; Leskelä, Markku; Repo, Timo
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	6
Pages of publication	1336
a	9.916 ± 0.001 Å
b	15.327 ± 0.001 Å
c	16.582 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	2520.2 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0447
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for significantly intense reflections	0.048
Weighted residual factors for all reflections included in the refinement	0.0511
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178646 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/57.	4075725.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075725.cif
50637	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075725, 4075726 via cif-deposit CGI script.	4075725.cif