Crystallography Open Database

Information card for entry 4076545

Preview

Coordinates	4076545.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H98 Cl4 Ge4 N8 P2 Si4
Calculated formula	C41 H98 Cl4 Ge4 N8 P2 Si4
Title of publication	Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
Authors of publication	West, Joseph K.; Stahl, Lothar
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	5
Pages of publication	2042
a	17.6548 ± 0.0007 Å
b	17.6548 ± 0.0007 Å
c	10.5683 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	3294.1 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	81
Hermann-Mauguin space group symbol	P -4
Hall space group symbol	P -4
Residual factor for all reflections	0.0232
Residual factor for significantly intense reflections	0.0218
Weighted residual factors for significantly intense reflections	0.0593
Weighted residual factors for all reflections included in the refinement	0.06
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178654 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/65.	4076545.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4076545.cif
51997	2012-04-07	../uploads/cif-deposit/cod/cif Adding structures of 4076536, 4076537, 4076538, 4076539, 4076540, 4076541, 4076542, 4076543, 4076544, 4076545 via cif-deposit CGI script.	4076545.cif