Crystallography Open Database

Information card for entry 4077271

Preview

Coordinates	4077271.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ru2(ap)4(C4TMS)
Formula	C58 H54 N8 Ru2 Si2
Calculated formula	C58 H54 N8 Ru2 Si2
Title of publication	Ru-σ-butadiynyl Complexes of the Tetraanilinopyridinatodiruthenium Core: Formation of a Bis-adduct
Authors of publication	Xu, Guolin; Ren, Tong
Journal of publication	Organometallics
Year of publication	2001
Journal volume	20
Journal issue	11
Pages of publication	2400
a	19.811 ± 0.002 Å
b	11.8642 ± 0.0012 Å
c	23.391 ± 0.002 Å
α	90°
β	90.717 ± 0.002°
γ	90°
Cell volume	5497.4 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.1095
Residual factor for significantly intense reflections	0.065
Weighted residual factors for significantly intense reflections	0.1582
Weighted residual factors for all reflections included in the refinement	0.1811
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178661 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/72.	4077271.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4077271.cif
54272	2012-04-24	cif/ Adding structures of 4077270, 4077271 via cif-deposit CGI script.	4077271.cif