Crystallography Open Database

Information card for entry 4079476

Preview

Coordinates	4079476.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H48 Bi2 N4 Si4
Calculated formula	C32 H48 Bi2 N4 Si4
Title of publication	Organobismuth(III) and Dibismuthine Complexes Bearing N,N′-Disubstituted 1,8-Diaminonaphthalene Ligand: Synthesis, Structure, and Reactivity
Authors of publication	Nekoueishahraki, Bijan; Samuel, Prinson P.; Roesky, Herbert W.; Stern, Daniel; Matussek, Julia; Stalke, Dietmar
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	18
Pages of publication	6697
a	18.0698 ± 0.0013 Å
b	12.2388 ± 0.0009 Å
c	17.9147 ± 0.0013 Å
α	90°
β	106.637 ± 0.002°
γ	90°
Cell volume	3796 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0247
Residual factor for significantly intense reflections	0.0163
Weighted residual factors for significantly intense reflections	0.0347
Weighted residual factors for all reflections included in the refinement	0.0371
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178683 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/94.	4079476.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4079476.cif
72447	2013-01-21	cif/ Adding structures of 4079469, 4079470, 4079471, 4079472, 4079473, 4079474, 4079475, 4079476 via cif-deposit CGI script.	4079476.cif