Crystallography Open Database

Information card for entry 4082384

Preview

Coordinates	4082384.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H22 O4 Si
Calculated formula	C15 H22 O4 Si
Title of publication	Synthesis of 4-Silacyclohexan-1-ones and (4-Silacyclohexan-1-yl)amines Containing the Silicon Protecting Groups MOP (4-Methoxyphenyl), DMOP (2,4-Dimethoxyphenyl), or TMOP (2,4,6-Trimethoxyphenyl): Versatile Si- and C-Functional Building Blocks for Synthesis
Authors of publication	Fischer, Markus; Burschka, Christian; Tacke, Reinhold
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	4
Pages of publication	1020
a	17.367 ± 0.003 Å
b	10.079 ± 0.0012 Å
c	19.795 ± 0.003 Å
α	90°
β	113.619 ± 0.016°
γ	90°
Cell volume	3174.7 ± 0.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0523
Residual factor for significantly intense reflections	0.041
Weighted residual factors for significantly intense reflections	0.1087
Weighted residual factors for all reflections included in the refinement	0.1149
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178712 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/23.	4082384.cif
104392	2014-03-11	cif/ Adding structures of 4082383, 4082384, 4082385, 4082386, 4082387, 4082388 via cif-deposit CGI script.	4082384.cif