Crystallography Open Database

Information card for entry 4083280

Preview

Coordinates	4083280.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C159 H123 Cl37 Fe2 P8 Pt4
Calculated formula	C159 H123 Cl37 Fe2 P8 Pt4
Title of publication	Imidazole Phosphines: Synthesis, Reaction Chemistry, and Their Use in SuzukiC,CCross-Coupling Reactions
Authors of publication	Milde, Bianca; Packheiser, Rico; Hildebrandt, Stefanie; Schaarschmidt, Dieter; Rüffer, Tobias; Lang, Heinrich
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	9
Pages of publication	3661
a	23.4813 ± 0.0007 Å
b	10.803 ± 0.0005 Å
c	34.7075 ± 0.0009 Å
α	90°
β	102.178 ± 0.003°
γ	90°
Cell volume	8606.1 ± 0.5 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.1617
Residual factor for significantly intense reflections	0.0826
Weighted residual factors for significantly intense reflections	0.1819
Weighted residual factors for all reflections included in the refinement	0.2224
Goodness-of-fit parameter for all reflections included in the refinement	0.943
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178721 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/32.	4083280.cif
113697	2014-05-13	cif/ Adding structures of 4083280 via cif-deposit CGI script.	4083280.cif