Crystallography Open Database

Information card for entry 4085428

Preview

Coordinates	4085428.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C111 H172 Li4 N8 Si4
Calculated formula	C111 H172 Li4 N8 Si4
Title of publication	Group 1 Complexes of an (Amido-amino)silane and Their Use in the Synthesis of the Bi(III) Amide, Bi(Me2Si{NAr}{N(H)Ar})Cl2(Ar = 2,6-i-Pr2C6H3)
Authors of publication	Schwamm, Ryan J.; Coles, Martyn P.; Fitchett, Christopher M.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	11
Pages of publication	2500
a	12.2412 ± 0.0003 Å
b	13.074 ± 0.0003 Å
c	20.0829 ± 0.0005 Å
α	105.704 ± 0.001°
β	93.758 ± 0.001°
γ	116.307 ± 0.001°
Cell volume	2708.84 ± 0.12 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0979
Residual factor for significantly intense reflections	0.061
Weighted residual factors for significantly intense reflections	0.1404
Weighted residual factors for all reflections included in the refinement	0.1585
Goodness-of-fit parameter for all reflections included in the refinement	0.98
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178743 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/54.	4085428.cif
141391	2015-07-09	cif/ Updating files of 4085428, 4085429, 4085430, 4085431 Original log message: Adding full bibliography for 4085428--4085431.cif.	4085428.cif
131170	2015-02-05	cif/ Adding structures of 4085428, 4085429, 4085430, 4085431 via cif-deposit CGI script.	4085428.cif