Crystallography Open Database

Information card for entry 4085646

Preview

Coordinates	4085646.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H26 Cu2 N4 O6
Calculated formula	C25 H20 Cu2 N4 O6
Title of publication	Synthesis of Multinuclear Copper Complexes Bridged by Diquinolylamidinates and Their Application to Copper-Catalyzed Coupling of Terminal Alkynes and Aryl, Allyl, and Benzyl Halides
Authors of publication	Nakane, Takayuki; Tanioka, Yuta; Tsukada, Naofumi
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	7
Pages of publication	1191
a	23.589 ± 0.01 Å
b	16.101 ± 0.006 Å
c	13.377 ± 0.005 Å
α	90°
β	101.844 ± 0.007°
γ	90°
Cell volume	4973 ± 3 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0767
Weighted residual factors for all reflections included in the refinement	0.1594
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178745 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/56.	4085646.cif
138298	2015-06-05	cif/ Updating files of 4085646, 4085647 Original log message: Adding full bibliography for 4085646--4085647.cif.	4085646.cif
134435	2015-03-27	cif/ Adding structures of 4085646, 4085647 via cif-deposit CGI script.	4085646.cif