Crystallography Open Database

Information card for entry 4085724

Preview

Coordinates	4085724.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H34 Cl2 O4 P2 Ru
Calculated formula	C26 H34 Cl2 O4 P2 Ru
Title of publication	Ruthenium Carbonyl Complexes Bearing Secondary Phosphine Oxides and Phosphinous Acids: Synthesis, Characterization, and Application in Catalysis
Authors of publication	Graux, Lionel V.; Giorgi, Michel; Buono, Gérard; Clavier, Hervé
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	10
Pages of publication	1864
a	21.5619 ± 0.0005 Å
b	13.5371 ± 0.0002 Å
c	19.8932 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	5806.5 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.1669
Residual factor for significantly intense reflections	0.0923
Weighted residual factors for significantly intense reflections	0.1237
Weighted residual factors for all reflections included in the refinement	0.1431
Goodness-of-fit parameter for all reflections included in the refinement	1.151
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176429 (current)	2016-02-13	cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary.	4085724.cif
140188	2015-07-05	cif/ Updating files of 4085723, 4085724, 4085725 Original log message: Adding full bibliography for 4085723--4085725.cif.	4085724.cif
136340	2015-05-13	cif/ Adding structures of 4085724 via cif-deposit CGI script.	4085724.cif