Crystallography Open Database

Information card for entry 4085816

Preview

Coordinates	4085816.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C15 H21 Al N2
Calculated formula	C15 H21 Al N2
Title of publication	Aluminum Alkyl Complexes Supported by Bidentate N,N Ligands: Synthesis, Structure, and Catalytic Activity for Guanylation of Amines
Authors of publication	Wei, Yun; Wang, Shaowu; Zhou, Shuangliu; Feng, Zhijun; Guo, Liping; Zhu, Xiancui; Mu, Xiaolong; Yao, Fangshi
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	10
Pages of publication	1882
a	6.965 ± 0.0011 Å
b	8.7743 ± 0.0014 Å
c	25.862 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	1580.5 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0687
Residual factor for significantly intense reflections	0.0419
Weighted residual factors for significantly intense reflections	0.0972
Weighted residual factors for all reflections included in the refinement	0.108
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4085816.cif
141374	2015-07-09	cif/ Updating files of 4085814, 4085815, 4085816, 4085817, 4085818, 4085819, 4085820 Original log message: Adding full bibliography for 4085814--4085820.cif.	4085816.cif
136840	2015-05-18	cif/ Adding structures of 4085814, 4085815, 4085816, 4085817, 4085818, 4085819, 4085820 via cif-deposit CGI script.	4085816.cif