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Information card for entry 4086722
Preview
| Coordinates | 4086722.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H30 Mg O2 |
|---|---|
| Calculated formula | C22 H30 Mg O2 |
| Title of publication | Mechanism of Alkyl Migration in Diorganomagnesium 2,6-Bis(imino)pyridine Complexes: Formation of Grignard-Type Complexes with Square-Planar Mg(II) Centers |
| Authors of publication | Sandoval, John J.; Palma, Pilar; Álvarez, Eleuterio; Cámpora, Juan; Rodríguez-Delgado, Antonio |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 18 |
| Pages of publication | 3197 |
| a | 9.37 ± 0.0007 Å |
| b | 9.0598 ± 0.0006 Å |
| c | 12.5313 ± 0.0008 Å |
| α | 90° |
| β | 100.684 ± 0.002° |
| γ | 90° |
| Cell volume | 1045.34 ± 0.12 Å3 |
| Cell temperature | 213 ± 2 K |
| Ambient diffraction temperature | 213 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0814 |
| Residual factor for significantly intense reflections | 0.0624 |
| Weighted residual factors for significantly intense reflections | 0.1747 |
| Weighted residual factors for all reflections included in the refinement | 0.2081 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.087 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 186942 (current) | 2016-10-05 | cif/ Adding structures of 4086721, 4086722, 4086723 via cif-deposit CGI script. |
4086722.cif |
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Users of the data should acknowledge the original authors of the
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