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Information card for entry 4086863
Preview
| Coordinates | 4086863.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H52 Co N2 O0.5 P |
|---|---|
| Calculated formula | C36 H52 Co N2 O0.5 P |
| Title of publication | Cobalt- and Iron-Catalyzed Isomerization‒Hydroboration of Branched Alkenes: Terminal Hydroboration with Pinacolborane and 1,3,2-Diazaborolanes |
| Authors of publication | Ogawa, Takahiko; Ruddy, Adam J.; Sydora, Orson L.; Stradiotto, Mark; Turculet, Laura |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| a | 12.149 ± 0.0004 Å |
| b | 22.1056 ± 0.0008 Å |
| c | 13.0832 ± 0.0005 Å |
| α | 90° |
| β | 101.58 ± 0.001° |
| γ | 90° |
| Cell volume | 3442.1 ± 0.2 Å3 |
| Cell temperature | 193 ± 2 K |
| Ambient diffraction temperature | 193 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0417 |
| Residual factor for significantly intense reflections | 0.0356 |
| Weighted residual factors for significantly intense reflections | 0.0945 |
| Weighted residual factors for all reflections included in the refinement | 0.0992 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 189675 (current) | 2017-01-01 | cif/ Adding structures of 4086858, 4086859, 4086860, 4086861, 4086862, 4086863 via cif-deposit CGI script. |
4086863.cif |
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Users of the data should acknowledge the original authors of the
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