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Information card for entry 4087589
Preview
| Coordinates | 4087589.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H21 Cr N O3 Pd |
|---|---|
| Calculated formula | C21 H21 Cr N O3 Pd |
| Title of publication | Stabilization of an Electron-Unsaturated Pd(I)‒Pd(I) Unit by Double Hemichelation |
| Authors of publication | Werlé, Christophe; Karmazin, Lydia; Bailly, Corinne; Ricard, Louis; Djukic, Jean-Pierre |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 12 |
| Pages of publication | 3055 |
| a | 8.352 ± 0.001 Å |
| b | 9.499 ± 0.001 Å |
| c | 13.15 ± 0.001 Å |
| α | 102.334 ± 0.001° |
| β | 94.604 ± 0.001° |
| γ | 102.481 ± 0.001° |
| Cell volume | 986.32 ± 0.17 Å3 |
| Cell temperature | 150 ± 0.1 K |
| Ambient diffraction temperature | 150 ± 0.1 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0606 |
| Residual factor for significantly intense reflections | 0.0533 |
| Weighted residual factors for significantly intense reflections | 0.1114 |
| Weighted residual factors for all reflections included in the refinement | 0.1146 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.208 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 236863 (current) | 2019-11-24 | cif/ Adding structures of 4087589, 4087590, 4087591, 4087592, 4087593, 4087594, 4087595 via cif-deposit CGI script. |
4087589.cif |
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Users of the data should acknowledge the original authors of the
structural data.