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Information card for entry 4087801
Preview
| Coordinates | 4087801.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H63 N3 P Si4 Y |
|---|---|
| Calculated formula | C35 H63 N3 P Si4 Y |
| Title of publication | Yttrium-Catalyzed Amine‒Silane Dehydrocoupling: Extended Reaction Scope with a Phosphorus-Based Ligand |
| Authors of publication | Nako, Adi E.; Chen, Wenyi; White, Andrew J. P.; Crimmin, Mark R. |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 17 |
| Pages of publication | 4369 |
| a | 15.154 ± 0.0006 Å |
| b | 12.962 ± 0.0005 Å |
| c | 22.1453 ± 0.0008 Å |
| α | 90° |
| β | 100.92 ± 0.004° |
| γ | 90° |
| Cell volume | 4271.2 ± 0.3 Å3 |
| Cell temperature | 173 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.064 |
| Residual factor for significantly intense reflections | 0.0394 |
| Weighted residual factors for significantly intense reflections | 0.0792 |
| Weighted residual factors for all reflections included in the refinement | 0.0876 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237010 (current) | 2019-11-24 | cif/ Adding structures of 4087799, 4087800, 4087801 via cif-deposit CGI script. |
4087801.cif |
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Users of the data should acknowledge the original authors of the
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